The diffraction pattern of nanocrystalline Ce0.9Zr0.1O2 was analyzed by whole powder pattern modeling, a recently proposed method for the study of line broadening. The main result in this typical case of study — the crystalline domain size distribution — matches closely the corresponding information obtained by transmission electron microscopy. Further information on nature and content of lattice defects is also discussed.
Grain size distribution of nanocrystalline systems
Scardi, Paolo;Leoni, Matteo;
2005-01-01
Abstract
The diffraction pattern of nanocrystalline Ce0.9Zr0.1O2 was analyzed by whole powder pattern modeling, a recently proposed method for the study of line broadening. The main result in this typical case of study — the crystalline domain size distribution — matches closely the corresponding information obtained by transmission electron microscopy. Further information on nature and content of lattice defects is also discussed.File in questo prodotto:
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