Pd nanocrystals were produced with uniform truncated-cube shape and a narrow size distribution, yielding controlled surface area fractions from low Miller index ({100}, {110}, {111}) crystalline facets. Details on the structure and morphology of the nanocrystals were obtained by combining X-ray powder diffraction line profile analysis, high-resolution transmission electron microscopy and surface electrochemistry based on Cu underpotential deposition.
Structure and morphology of shape-controlled Pd nanocrystals / Solla Gullon, Jose; Garnier, Emmanuel; Feliu, Juan M.; Leoni, Matteo; Leonardi, Alberto; Scardi, Paolo. - In: JOURNAL OF APPLIED CRYSTALLOGRAPHY. - ISSN 0021-8898. - ELETTRONICO. - 48:5(2015), pp. 1534-1542. [10.1107/S1600576715015964]
Structure and morphology of shape-controlled Pd nanocrystals
Leoni, Matteo;Leonardi, Alberto;Scardi, Paolo
2015-01-01
Abstract
Pd nanocrystals were produced with uniform truncated-cube shape and a narrow size distribution, yielding controlled surface area fractions from low Miller index ({100}, {110}, {111}) crystalline facets. Details on the structure and morphology of the nanocrystals were obtained by combining X-ray powder diffraction line profile analysis, high-resolution transmission electron microscopy and surface electrochemistry based on Cu underpotential deposition.| File | Dimensione | Formato | |
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